The following standard experiments are offered:

Service at 400 or 600 MHz by staff:

¹H, ¹³C, ³¹P, HMQC, HSQC, HMBC, COSY, TOCSY, NOESY and ROESY
Further methods (1D and 2D) as well as measurments of other nucleus, if required, can be offered after consultation with us.

Remark: For an efficient execution of orders, the following amounts of substance are desirable:

• ¹H: 0.03 mmol
• ¹³C: 0.1 mmol
• ³¹P: 0.1 mmol

These amounts must be soluble in 0.8 ml of the desired solvent. Please check the solubility!

How to prepare your samples, you can find here: "Tips for preparing a NMR-Tube".

You will get order forms here:

• PDF - File

Labels for the NMR tubes can you get here :

• Labels for workgroup
  
• Labels for  Praktika

Self service at devices downstairs:

After receiving instructions by our staff, you can measure by yourself on the AVA300, AVA400neu, AVA400stud and AVA500. Only longterm users listed on the workgroup's website with a fixed workplace (graduate students working on master/PhD thesis, WHKs, exchange students, guest scientist etc.) will receive instructions. For short or less frequent usage, use our staff's service or ask your colleagues/supervisors to submit them for you.

Some available experiments: ¹H, ¹³C{¹H} (multiplicities via DEPT), ³¹P{¹H}, ³¹P, ¹⁹F{¹H} and ¹⁹F, HSQC, HMBC, Cosy, Noesy, Roesy und Tocsy.

For this purpose you can find details in our instruction for Icon-NMR (menu "Internal")

Access to the spectra data: 

The raw data (FID's) are available in the network of the university. In case of WINDOWS standard installations in the Faculty Chemistry and Pharmacy, you can find the raw data in the dirctory I:\NMRSPEC  (synonymous with \\Titan-DPS009\DPS009\CHEMIE\ZA\messdat\nmrspec) accordingly to the names of the devices (AVA300, AVA400, AVA600, ...). The data will be available for users to copy for 90 days. Older data will be moved in an archive and are not accessible by public. Please backup your data as soon as possible (make sure you backup the whole data folder with the raw FID, not just the processed spectra from your software!)